MICROSTRUCTURE EVOLUTION OF AN Al-Cu ALLOY IN THIN-SAMPLE POLYCRYSTALLINE SOLIDIFICATION: IN SITU SYNCHROTON X-RAY RADIOGRAPHY IMAGING AND FULL-SCALE PHASE-FIELD SIMULATIONS

18 Jun 2019, 15:00
20m
P4 (IMLAUER HOTEL PITTER SALZBURG)

P4

IMLAUER HOTEL PITTER SALZBURG

Rainerstraße 6, 5020 Salzburg, Austria
Oral Presentation Dendritic microstructure

Speaker

Tong Zhao Gong (Institute of Metal Research, Chinese Academy of Sciences)

Description

The growth dynamics of multiple equiaxed dendrites in a thin metallic sample is studied using *in situ* synchrotron X-ray imaging of Al-4 wt.%Cu alloy solidification experiments and corresponding full-scale three-dimensional (3-D) phase-field (PF) simulations. The tip growth velocity *V*, tip radius *ρ*, the secondary dendritic arm spacing (SDAS) *λ*$_2$ and the total solid fraction *f*$_s$, are analyzed systematically in a relatively large range of cooling rate *R*$_c$. Through an in-depth comparison of the growth dynamics with experiments, including the tip velocity and the primary arm length, the nucleation undercooling for each grain is estimated. Quantitative agreements in *V* of several selected grains and *f*$_s$ between experiments and simulations have been achieved. The tip velocity, followed by free growth from the melt that is cooled continuously at constant *R*$_c$, decreases first at the very beginning of solidification in both experiments and simulations. Subsequently, *V* increases up to a peak value until the grains interact with each other by solutal effect. Moreover, an oscillation growth of the dendritic tip is observed during the soft-impinged growth stage in both experiments and simulations, featured by an acceleration of *V* after it goes down to a minimum from the peak value. With increasing *R*$_c$, *V* will be enlarged while *ρ* will be reduced, due to the narrowed solute boundary layer ahead of the tip. Furthermore, *ρ* and *λ*$_2$ show good agreements between simulations and dendrite growth theories, with *ρ* $\sim$ *V*$^{-1/2}$ and *λ*$_2$ $\sim$ *R*$_c^{-1/3}$. However, experimental measurements of *λ*$_2$ are generally larger than *λ*$_2$ in PF simulations, and this discrepancy could be attributed to liquid convection in experiments, despite the thin sample configuration. We incorporate liquid flow dynamics into the computationally less-demanding 2-D PF simulations. It has been found that with the gravity-driven convection the sidebranches are more developed and coarsened, thereby enlarging the spacing between the secondary arms.
Speaker Country China

Author

Tong Zhao Gong (Institute of Metal Research, Chinese Academy of Sciences)

Co-authors

Prof. Dian Zhong Li (Institute of Metal Research, Chinese Academy of Sciences) Prof. Henri Hguyen-Thi (Aix-Marseille Université, IM2NP, Campus scientifique Saint-Jérôme) Prof. Yun Chen (Institute of Metal Research, Chinese Academy of Sciences)

Presentation materials