IN SITU AND OPERANDO SYNCHROTRON QUANTIFICATION OF PRIMARY SOLIDIFICATION IN IN713C DURING ADDITIVE MANUFACTURING

20 Jun 2019, 18:14
1m
IMLAUER HOTEL PITTER SALZBURG

IMLAUER HOTEL PITTER SALZBURG

Rainerstraße 6, 5020 Salzburg, Austria

Speaker

Samuel Clark (University College London)

Description

Laser Additive Manufacturing (LAM) can directly produce near-net-shape metallic components using commercial alloy powders. However, primary solidification during LAM is far from equilibrium due to the ultra-fast laser-powder interaction (<50 ms), mixing of solutes during melting and micro-segregation upon rapid solidification. Our understanding of these phenomena and the resultant microstructural features formed cannot be fully elucidated using traditional a posteriori characterization, necessitating in situ and operando characterization. We have developed a LAM Process Replicator (LAMPR) that allows real and reciprocal space synchrotron imaging of LAM. The X-ray diffraction study presented exploits the quasi-steady-state and layer-wise AM to enable the detection of the primary solidification of tracks under conditions distant from the near equilibrium transformations observed from conventional processing. This is complemented with in situ and operando x-ray imaging of the same process. The results can be used to help design new alloys and guide the optimisation of processing parameters to exploit the full potential of LAM.
Speaker Country United Kingdom

Author

Samuel Clark (University College London)

Co-authors

Dr Alexander Rack (European Synchrotron Radiation Facility) Prof. Andre Phillion (McMaster University) Dr Chu Lun Alex Leung (University College London) Dr Jon Willmott (University of Sheffield) Mr Leigh Stanger (University of Sheffield) Ms Lorna Sinclair (University of Manchester) Dr Margie Olbinado (European Synchrotron Radiation Facility) Dr Mohammed Azeem (University College London) Prof. Peter Lee (University College London) Dr Robert Atwood (Diamond Light Source) Mr Sebastian Marussi (University of Manchester) Dr Veijo Honkimaki (European Synchrotron Radiation Facility) Dr Yunhui Chen (University College London)

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