13–17 Sept 2021 Virtual Conference
Virtual
Europe/Vienna timezone
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In-situ tensile tests for mechanical characterization of steels with complex microstructure

13 Sept 2021, 14:40
20m
Room 6

Room 6

Oral Presentation B7. Material testing, characterisation and modelling (incl. C8) B7_Material testing, characterisation and modelling

Speaker

Mr Maxime Mollens (EDF R&D - LMT ENS Paris-Saclay)

Description

Monitoring pressurized water reactors casted duplex stainless steel parts is of interest in long-term operation of nuclear power plants. It has been shown that these components are subjected to ageing when held at their operating temperature. In the long run, thermal ageing results in embrittlement due to a microstructural evolution of one of the two phases constituting duplex steels. Kinetics and impact of ageing on fracture mechanics have been studied to a great extent. However, deformation and damage mechanisms leading to fracture are not yet fully understood owing to the complexity of duplex steels microstructure. Resorting to traditionally used global energy balance methods (J-Δa curves) is not sufficient to understand the primordial role of microstructure in the evolution of mechanical properties with thermal ageing. In this context, a microstructure characterization is performed jointly to in-situ mechanical characterization to build a consistent micromechanical model taking the multi scale aspect of the microstructure into account. Eventually, the model must provide a fine description of the material mechanical behaviour taking into account the aged state
In order to relate crystal plasticity finite element computations to experimental observations, digital images correlation (DIC) is used to provide full-field measurements. They must be consistent with the deformation mechanisms of the studied steels and be accurate enough to capture small deformation mechanisms occurring in each phase (at a micrometre scale) and the resulting displacements at the larger scale of the microstructure (several millimetres). Duplex steels natural texture is not sufficient to carry out digital images correlation. Thus, an adequate speckle pattern was designed and deposited through electron beam lithography.

Figure 1: a) Austenite crystallographic orientation map ; b) Speckle deposited by electron beam lithography used for SEM DIC; c) principal strain field obtained at 2.7% macroscopic deformation

Speaker Country France

Author

Mr Maxime Mollens (EDF R&D - LMT ENS Paris-Saclay)

Co-authors

Mr Adrien Guery (EDF R&D) Mr François Hild (LMT ENS Paris-Saclay) Mr Stéphane Roux (LMT ENS Paris-Saclay)

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