13–17 Sept 2021 Virtual Conference
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Influence of microstructure on the multicaloric effect of Ni-Mn-based metamagnetic shape-memory alloys

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3m
Virtual

Virtual

Poster A6. Characterisation of functional materials A6_Poster Session

Speaker

Mr Lukas Pfeuffer (Technical University of Darmstadt)

Description

Ni-Mn-based metamagnetic shape-memory alloys exhibit outstanding caloric effects in the vicinity of martensitic transformations driven by magnetic fields, uniaxial load or hydrostatic pressure. However, the application in refrigeration devices is hindered by energy losses and/or irreversibilities during cyclic operation which originate from a large inherent thermal hysteresis of the non-diffusional phase transformation. A promising way to improve cyclic performance is a simultaneous or sequential combination of more than one external stimulus. We have recently presented that a sequential application of magnetic field and uniaxial load can even make use of thermal hysteresis. In this so called “exploiting-hysteresis cycle”, the shape-memory alloy initially undergoes a magnetic-field-induced reverse martensitic transformation from low-magnetization martensite to high-magnetization austenite [1]. In consequence of the large thermal hysteresis, the material is trapped in the high-magnetization austenite even after the magnetic field is removed. To ensure cyclability, the back transformation to the original martensite state is driven by uniaxial load.

We studied the correlation of microstructure and the caloric response to magnetic fields, uniaxial load and their combination in an "exploiting-hysteresis cycle" exemplarily for the metamagnetic shape-memory alloy Ni-Mn-In. We reveal a significant effect of grain orientation on the stress-induced martensitic transformation by correlating temperature-dependent XRD and SEM-EBSD data. By strain measurements in static and pulsed magnetic fields a crucial role of microstructure on the field-induced transformation dynamics is demonstrated [2]. We show that for a tailored microstructure the maximum cyclic effect in 1.9 T can be raised by more than 200 % when a moderate sequential stress of 59 MPa is applied.

[1] Gottschall et al.; Nature Materials 17, 929-934 (2018)

[2] Pfeuffer et al.; Physical Review Materials 4, 111401 (2020)

Speaker Country Germany

Author

Mr Lukas Pfeuffer (Technical University of Darmstadt)

Co-authors

Adrià Gràcia-Condal (Universitat de Barcelona) Andreas Taubel (Technical University of Darmstadt) Antoni Planes (Universitat de Barcelona) David Koch (Technical University of Darmstadt) Enrico Bruder (Technical University of Darmstadt) Franziska Scheibel (Technical University of Darmstadt) Jonas Lemke (Technical University of Darmstadt) Karsten Durst (Technical University of Darmstadt) Konstantin Skokov (Technical University of Darmstadt) Lluís Mañosa (Universitat de Barcelona) Oliver Gutfleisch (Technical University of Darmstadt) Semih Ener (Technical University of Darmstadt) Tino Gottschall (Helmholtz-Zentrum Dresden-Rossendorf) Tom Faske (Technical University of Darmstadt)

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